7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

Base Information

Chemical Name:7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride
CAS No.:1338797-40-2
Molecular Formula:C₁₇H₁₆BrNO*ClH
Molecular Weight:366.685
Hs Code.:

Synonyms:7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

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Chemical Property of 7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

Chemical Property:

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Technology Process of 7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

There total 12 articles about 7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1338797-31-1
4-bromo-7-(tert-butoxycarbonylamino)-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one

: 1338797-40-2
7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 20 ℃; for 48h;
DOI:10.1016/j.bmc.2011.06.089

Reference yield:

: C₂₃H₂₉BrO₂Si

: 1338797-40-2
7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride / pyridine / 5 h / 25 °C

1.2: 2 h / 25 °C

2.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / methanol / 2 h / -30 - 25 °C

3.1: sodium carbonate / methanol / 25 °C

3.2: 2 h / 25 °C

4.1: hydrogenchloride / diethyl ether / 25 °C

With hydrogenchloride; sodium tetrahydroborate; cobalt(II) chloride hexahydrate; hydroxylamine hydrochloride; sodium carbonate; In pyridine; methanol; diethyl ether;
DOI:10.3390/molecules23102607

Reference yield:

: 1338797-52-6
C₁₇H₁₈BrNO

: 1338797-40-2
7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / methanol / 25 °C

1.2: 2 h / 25 °C

2.1: hydrogenchloride / diethyl ether / 25 °C

With hydrogenchloride; sodium carbonate; In methanol; diethyl ether;
DOI:10.3390/molecules23102607