4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

Base Information

Chemical Name:4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde
CAS No.:366815-53-4
Molecular Formula:C₂₅H₃₀N₄O₃
Molecular Weight:434.538
Hs Code.:

Synonyms:4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

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Chemical Property of 4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

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Technology Process of 4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

There total 6 articles about 4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 100-44-7
benzyl chloride

: 366815-50-1
4-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

: 366815-53-4
4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

Guidance literature:: With potassium carbonate; In acetonitrile; Reflux;
DOI:10.1021/jo902504d

Reference yield: 75.0%

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 112498-58-5
4-benzyl-1,4,7-triazacyclononane-1-carbaldehyde

: 366815-53-4
4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

Guidance literature:: With sodium carbonate; In acetonitrile; for 72h; Heating;
DOI:10.1021/ol016291d

Reference yield:

: 100-39-0
benzyl bromide

: 366815-53-4
4-benzyl-7-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-[1,4,7]triazonane-1-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0.5 h

2: 2.30 g / H₂O / 4 h / Heating

3: 75 percent / sodium carbonate / acetonitrile / 72 h / Heating

With water; sodium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol016291d