Technology Process of C34H38N3(1+)*I(1-)
There total 7 articles about C34H38N3(1+)*I(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 120h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); triethylamine; formic acid / N,N-dimethyl-formamide / 4 h / 70 °C / Inert atmosphere
2: cyclohexene; palladium 10% on activated carbon / ethanol / 19 h / Inert atmosphere; Reflux
3: CHIRALPAK? IA column / diethylamine; acetonitrile / Resolution of racemate
4: ethanol / 23 h / 100 °C / Autoclave
5: triethylamine / tetrahydrofuran / 4 h / 20 °C
6: triethylamine / chloroform / 7.5 h / 20 °C
7: potassium carbonate / methanol / 120 h / 20 °C / Inert atmosphere
With
formic acid; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); palladium 10% on activated carbon; potassium carbonate; triethylamine; cyclohexene;
In
tetrahydrofuran; methanol; ethanol; chloroform; diethylamine; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ethanol / 23 h / 100 °C / Autoclave
2: triethylamine / tetrahydrofuran / 4 h / 20 °C
3: triethylamine / chloroform / 7.5 h / 20 °C
4: potassium carbonate / methanol / 120 h / 20 °C / Inert atmosphere
With
potassium carbonate; triethylamine;
In
tetrahydrofuran; methanol; ethanol; chloroform;
![(-)-dimethyl-[5-(8-trityl-8-azabicyclo[3.2.1]oct-6-yl)pyridine-2-yl]amine](/Databaselist/images/loading.webp)
