N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

Base Information

Chemical Name:N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine
CAS No.:1332371-57-9
Molecular Formula:C₂₀H₂₅NSi
Molecular Weight:307.511
Hs Code.:

Synonyms:N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

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Chemical Property of N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

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Technology Process of N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

There total 2 articles about N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1126942-58-2
chloro(dimethyl)(2-methyl-1H-inden-7-yl)silane

: 108-69-0
3,5-dimethylaminoaniline

: 1332371-57-9
N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

Guidance literature:: 3,5-dimethylaminoaniline; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 4h;

chloro(dimethyl)(2-methyl-1H-inden-7-yl)silane; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 12h;

Reference yield:

: 880652-93-7
4⁽⁷⁾-bromo-2-methyl-1⁽³⁾H-indene

: 1332371-57-9
N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylene dibromide; magnesium / tetrahydrofuran / 0.5 h / Reflux

1.2: 12 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 4 h / 0 - 20 °C

2.2: 12 h / -40 - 20 °C

With n-butyllithium; magnesium; ethylene dibromide; In tetrahydrofuran; hexane;

Reference yield: 59.0%

: 1332371-57-9
N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine

: 7550-45-0
titanium tetrachloride

: {η⁵:η¹-N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methylinden-4-yl)silanamido}titanium dichloride

Guidance literature:: N-(3,5-dimethylphenyl)-1,1-dimethyl-1-(2-methyl-1H-inden-7-yl)silanamine; With n-butyllithium; In diethyl ether; hexane; at 20 ℃; for 12h;

titanium tetrachloride; In diethyl ether; hexane; at 0 - 20 ℃; for 12h;