N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

Base Information

Chemical Name:N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide
CAS No.:1092394-66-5
Molecular Formula:C₁₆H₁₃N₅O₄
Molecular Weight:339.31
Hs Code.:

Synonyms:N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

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Technology Process of N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

There total 1 articles about N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1092394-65-4
6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-amine

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 1092394-66-5
N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

Guidance literature:: With triethylamine; In N,N-dimethyl acetamide; at 20 ℃; for 15h;

Reference yield: 25.0%

: 1092394-66-5
N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

: 1092391-99-5
N-[6-(3-aminophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

Guidance literature:: N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide; With hydroxylamine hydrochloride; zinc; In methanol; for 3h; Heating / reflux;

With hydrogenchloride; iron; In ethanol; water; for 1h; Heating / reflux;

Reference yield:

: 1092394-66-5
N-[6-(3-nitrophenoxy)[1,2,4]triazolo[1,5-a]pyridin-2-yl]cyclopropanecarboxamide

: 1092391-51-9
N-[3-({2-[(cyclopropylcarbonyl)amino][1,2,4]triazolo[1,5-a]pyridin-6-yl}oxy)phenyl]-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride; zinc / methanol / 3 h / Heating / reflux

1.2: 1 h / Heating / reflux

2.1: oxalyl dichloride / 6-methyl-2-pyridinecarboxylic acid / tetrahydrofuran / 1 h / 20 °C

2.2: 15 h / 20 °C

With oxalyl dichloride; hydroxylamine hydrochloride; zinc; 6-methyl-2-pyridinecarboxylic acid; In tetrahydrofuran; methanol;