benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

Base Information

Chemical Name:benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate
CAS No.:1374138-03-0
Molecular Formula:C₃₅H₄₇NO₄Si
Molecular Weight:573.848
Hs Code.:

Synonyms:benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

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Chemical Property of benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

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Technology Process of benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

There total 10 articles about benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374138-02-9
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

: 1374138-03-0
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

Guidance literature:: benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate; With 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 0.166667h; Molecular sieve;

With tetrapropylammonium perruthennate; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: C₂₂H₃₃NO₂Si*ClH

: 1374138-03-0
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / methanol / 0.5 h / 20 °C

1.2: 20 °C

2.1: sodium hydrogencarbonate / chloroform; water / 1 h / 20 °C

3.1: 4-methylmorpholine N-oxide / dichloromethane / 0.17 h / 20 °C / Molecular sieve

3.2: 3 h / 20 °C

With sodium hydrogencarbonate; acetic acid; 4-methylmorpholine N-oxide; In methanol; dichloromethane; chloroform; water;

Reference yield:

: 85535-55-3
(S)-di-tert-butyl (6-hydroxyhexane-1,5-diyl)dicarbamate

: 1374138-03-0
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-oxohexan-2-yl](3-methylbutyl)carbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / dichloromethane / 0 - 20 °C

2.1: sodium bromate; ruthenium(IV) oxide hydrate / ethyl acetate; water / 20 - 55 °C

3.1: water; sodium tetrahydroborate / isopropyl alcohol / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

5.1: acetic acid / methanol / 0.5 h / 20 °C

5.2: 20 °C

6.1: sodium hydrogencarbonate / chloroform; water / 1 h / 20 °C

7.1: 4-methylmorpholine N-oxide / dichloromethane / 0.17 h / 20 °C / Molecular sieve

7.2: 3 h / 20 °C

With 1H-imidazole; hydrogenchloride; sodium bromate; sodium tetrahydroborate; ruthenium(IV) oxide hydrate; water; sodium hydrogencarbonate; acetic acid; 4-methylmorpholine N-oxide; In 1,4-dioxane; methanol; dichloromethane; chloroform; water; ethyl acetate; isopropyl alcohol;