benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

Base Information

Chemical Name:benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate
CAS No.:1374138-02-9
Molecular Formula:C₃₅H₄₉NO₄Si
Molecular Weight:575.864
Hs Code.:

Synonyms:benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

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Chemical Property of benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

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Technology Process of benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

There total 9 articles about benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374138-01-8
(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

: 501-53-1,94274-21-2
benzyl chloroformate

: 1374138-02-9
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

Guidance literature:: With sodium hydrogencarbonate; In chloroform; water; at 20 ℃; for 1h;

Reference yield:

: 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride

: 1374138-02-9
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: lithium borohydride / tetrahydrofuran / 2 h / 0 - 50 °C

2.2: 0 - 20 °C

3.1: 1H-imidazole / dichloromethane / 0 - 20 °C

4.1: sodium bromate; ruthenium(IV) oxide hydrate / ethyl acetate; water / 20 - 55 °C

5.1: water; sodium tetrahydroborate / isopropyl alcohol / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

7.1: acetic acid / methanol / 0.5 h / 20 °C

7.2: 20 °C

8.1: sodium hydrogencarbonate / chloroform; water / 1 h / 20 °C

With 1H-imidazole; hydrogenchloride; sodium bromate; sodium tetrahydroborate; lithium borohydride; ruthenium(IV) oxide hydrate; water; sodium hydrogencarbonate; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; ethyl acetate; isopropyl alcohol;

Reference yield:

: 85535-55-3
(S)-di-tert-butyl (6-hydroxyhexane-1,5-diyl)dicarbamate

: 1374138-02-9
benzyl [(2S)-1-{[tert-butyl(diphenyl)silyl]oxy}-6-hydroxyhexan-2-yl](3-methylbutyl)carbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 0 - 20 °C

2.1: sodium bromate; ruthenium(IV) oxide hydrate / ethyl acetate; water / 20 - 55 °C

3.1: water; sodium tetrahydroborate / isopropyl alcohol / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

5.1: acetic acid / methanol / 0.5 h / 20 °C

5.2: 20 °C

6.1: sodium hydrogencarbonate / chloroform; water / 1 h / 20 °C

With 1H-imidazole; hydrogenchloride; sodium bromate; sodium tetrahydroborate; ruthenium(IV) oxide hydrate; water; sodium hydrogencarbonate; acetic acid; In 1,4-dioxane; methanol; dichloromethane; chloroform; water; ethyl acetate; isopropyl alcohol;