ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

Base Information

Chemical Name:ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate
CAS No.:858917-00-7
Molecular Formula:C₂₃H₃₈O₅Si
Molecular Weight:422.637
Hs Code.:

Synonyms:ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

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Chemical Property of ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

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Technology Process of ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

There total 10 articles about ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 439143-40-5
ethyl (2E)-(5R)-5-hydroxy-6-[(4-methoxyphenyl)-methoxy]-3-methylhex-2-enoate

: 858917-00-7
ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 18h;
DOI:10.1002/anie.200500564

Reference yield:

: 121289-23-4
p-methoxybenzyloxyacetaldehyde

: 858917-00-7
ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 6-bis[(4R)-4-phenyl-2-oxazolin-2-yl]pyridine; CuCl₂; AgSbF₆ / CH₂Cl₂ / 4 h / -78 °C

2: 89 percent / imidazole / dimethylformamide / 18 h

With 1H-imidazole; silver hexafluoroantimonate; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine; copper dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200500564

Reference yield:

: 131489-39-9
1-<(trimethylsilyl)oxy>-1-ethoxy-3-methyl-1,3-butadiene

: 858917-00-7
ethyl (2E,5R)-6-[(4-methoxyphenyl)methoxy]-3-methyl-5-(1,1,2,2-tetramethyl-1-silapropoxy)hex-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 6-bis[(4R)-4-phenyl-2-oxazolin-2-yl]pyridine; CuCl₂; AgSbF₆ / CH₂Cl₂ / 4 h / -78 °C

2: 89 percent / imidazole / dimethylformamide / 18 h

With 1H-imidazole; silver hexafluoroantimonate; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine; copper dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200500564