3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

Base Information

Chemical Name:3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester
CAS No.:325962-13-8
Molecular Formula:C₃₀H₄₁NO₁₃S
Molecular Weight:655.72
Hs Code.:

Synonyms:3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

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Chemical Property of 3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

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Technology Process of 3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

There total 1 articles about 3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.2%

: 73159-07-6
allyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,54-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid methyl ester

: 100-53-8
phenylmethanethiol

: 325962-13-8
3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 80 ℃; for 1.5h;
DOI:10.1016/S0008-6215(00)00247-0

Reference yield: 78.1%

: 325962-13-8
3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

: 325962-14-9
3-benzylthiopropyl 5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid methyl ester

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h;
DOI:10.1016/S0008-6215(00)00247-0

Reference yield:

: 325962-13-8
3-benzylthiopropyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid metyl ester

: 3-benzylthiopropyl 5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 78.1 percent / NaOMe / methanol / 2 h / 20 °C

2: 100 percent / aq. NaOH / 1 h / 20 °C

With sodium hydroxide; sodium methylate; In methanol;
DOI:10.1016/S0008-6215(00)00247-0