C₆₁H₇₃NO₁₅Si

Base Information

Chemical Name:C₆₁H₇₃NO₁₅Si
CAS No.:153145-54-1
Molecular Formula:C₆₁H₇₃NO₁₅Si
Molecular Weight:1088.33
Hs Code.:

C<sub>61</sub>H<sub>73</sub>NO<sub>15</sub>Si

Synonyms:C₆₁H₇₃NO₁₅Si

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Chemical Property of C₆₁H₇₃NO₁₅Si

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Technology Process of C₆₁H₇₃NO₁₅Si

There total 25 articles about C₆₁H₇₃NO₁₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₅₆O₉Si₂

: 153145-54-1
C₆₁H₇₃NO₁₅Si

Guidance literature:: Multi-step reaction with 20 steps

2: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

3: 100 percent / p-TsOH

4: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

5: acid

6: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

7: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

8: 95 percent / CH₂Cl₂ / 15 h / -45 °C

9: 63 percent / Burgess' reagent

10: 100 percent / pyridine

11: 65 percent / OsO₄

12: DBU / toluene / 2 h / 105 °C

13: 75 percent / pyridine, DMAP / 24 h / 25 °C

14: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

15: tetrahydrofuran / 0.17 h / -78 °C

16: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

17: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

18: pyridine, DMAP / 20 h / 25 °C

19: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

20: 1.) LHMDS / 1.) THF, 2.) THF, 0 deg C, 1 h

With pyridine; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-54-1
C₆₁H₇₃NO₁₅Si

Guidance literature:: Multi-step reaction with 22 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

16: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

17: tetrahydrofuran / 0.17 h / -78 °C

18: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

19: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

20: pyridine, DMAP / 20 h / 25 °C

21: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

22: 1.) LHMDS / 1.) THF, 2.) THF, 0 deg C, 1 h

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 153145-56-3
C₃₃H₅₆O₈Si₂

: 153145-54-1
C₆₁H₇₃NO₁₅Si

Guidance literature:: Multi-step reaction with 21 steps

1: KMnO₄, KH₂PO₄

3: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

4: 100 percent / p-TsOH

5: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

6: acid

7: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

8: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

9: 95 percent / CH₂Cl₂ / 15 h / -45 °C

10: 63 percent / Burgess' reagent

11: 100 percent / pyridine

12: 65 percent / OsO₄

13: DBU / toluene / 2 h / 105 °C

14: 75 percent / pyridine, DMAP / 24 h / 25 °C

15: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

16: tetrahydrofuran / 0.17 h / -78 °C

17: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

18: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

19: pyridine, DMAP / 20 h / 25 °C

20: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

21: 1.) LHMDS / 1.) THF, 2.) THF, 0 deg C, 1 h

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;