di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

Base Information

Chemical Name:di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate
CAS No.:1256550-62-5
Molecular Formula:C₁₈H₂₇NO₆
Molecular Weight:353.415
Hs Code.:

Synonyms:di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

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Chemical Property of di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

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Technology Process of di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

There total 5 articles about di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1304014-09-2
di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

: 1256550-62-5
di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1021/ol200808q

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1256550-62-5
di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C

2: 1H-imidazole / acetonitrile / 1 h / 20 °C / Inert atmosphere

3: dmap / acetonitrile / 50 °C

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 0 °C

With 1H-imidazole; dmap; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/ol200808q

Reference yield:

: 1304014-07-0
tert-butyl 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethylcarbamate

: 1256550-62-5
di(tert-butyl) 2-(3,4-dihydroxyphenyl)ethyliminodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / acetonitrile / 50 °C

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 0 °C

With dmap; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol200808q