di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

Base Information

Chemical Name:di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate
CAS No.:1304014-09-2
Molecular Formula:C₃₀H₅₅NO₆Si₂
Molecular Weight:581.941
Hs Code.:

Synonyms:di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

Chemical Property:

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Technology Process of di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

There total 4 articles about di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1304014-07-0
tert-butyl 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethylcarbamate

: 1304014-09-2
di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

Guidance literature:: With dmap; In acetonitrile; at 50 ℃;
DOI:10.1021/ol200808q

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1304014-09-2
di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C

2: 1H-imidazole / acetonitrile / 1 h / 20 °C / Inert atmosphere

3: dmap / acetonitrile / 50 °C

With 1H-imidazole; dmap; sodium hydrogencarbonate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/ol200808q

Reference yield:

: 37034-31-4
N-(tert-butoxycarbonyl)dopamine

: 1304014-09-2
di(tert-butyl) 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyliminodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / acetonitrile / 1 h / 20 °C / Inert atmosphere

2: dmap / acetonitrile / 50 °C

With 1H-imidazole; dmap; In acetonitrile;
DOI:10.1021/ol200808q