Technology Process of C24H32O5
There total 14 articles about C24H32O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
L-Selectride;
In
tetrahydrofuran;
for 1h;
cooling;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / boric acid; H2 / W-2 Raney nickel / H2O; methanol / 6 h / 20 °C
2: 89 percent / L-selectride / tetrahydrofuran / 1 h / cooling
With
hydrogen; boric acid; L-Selectride;
W-2 Raney nickel;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.28 g / KF / propan-2-ol / 20 °C
2: 95 percent / methanesulfochloride; triethylamine / CH2Cl2 / 0.08 h / 0 °C
3: zinc; aq. acetic acid / tetrahydrofuran / 0.08 h / 0 °C
4: 592 mg / sodium hypochlorite / H2O; CH2Cl2 / 5 h / 20 °C
5: 85 percent / boric acid; H2 / W-2 Raney nickel / H2O; methanol / 6 h / 20 °C
6: 89 percent / L-selectride / tetrahydrofuran / 1 h / cooling
With
potassium fluoride; sodium hypochlorite; hydrogen; boric acid; L-Selectride; acetic acid; triethylamine; zinc;
W-2 Raney nickel;
In
tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/ol0701013