N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

Base Information

Chemical Name:N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate
CAS No.:1207738-87-1
Molecular Formula:BF₄*C₄₂H₄₂FeN₂PS
Molecular Weight:780.5
Hs Code.:

Synonyms:N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

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Chemical Property of N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

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Technology Process of N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

There total 1 articles about N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 5,6-dimethyl-1-(2,4,6-trimethylbenzyl)-1H-benzo[d]imidazole

: tetrafluoroboric acid

: 954149-64-5
[1'-(diphenylthiophosphanyl)ferrocen-1-yl]methanol

: 1207738-87-1
N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

Guidance literature:: In diethyl ether; dichloromethane; (Ar), HBF4 in Et2O added quikly to soln. of Fe complex in degassed CH2Cl2, treated immediately with 1.5 equiv. of ligand; washed (aq.HCl, H2O, satd.aq.NaHCO3, H2O), org. phase dried (MgSO4), concd.(vac.), chromy.(silica gel - CH2Cl2/acetone 9:1), elem. anal.;
DOI:10.1002/ejic.200801163

Reference yield: 85.0%

: 1207738-87-1
N-[(1-diphenylthiophosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

: 1207738-92-8
N-[(1-diphenylphosphanylferrocen-1'-yl)methyl]-N'-[(2,4,6-trimethylphenyl)methyl]-5,6-dimethylbenzimidazolium tetrafluoroborate

Guidance literature:: nickel; In acetonitrile; (Ar), Raney Ni washed with degassed CH3OH, Et2O, CH3CN, treated with soln. of Fe complex in CH3CN, stirred at room temp. for 24 h; filtered (celite), rinzed (CH3CN), concd., dried (vac.), elem. anal.;
DOI:10.1002/ejic.200801163