(2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

Base Information

Chemical Name:(2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide
CAS No.:929208-88-8
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

Synonyms:(2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

Suppliers and Price of (2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

Chemical Property:

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Technology Process of (2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

There total 4 articles about (2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30725-00-9
2,3-O-isopropylidene-D-ribonic-γ-lactone

: 929208-88-8
(2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Ag₂O / dimethylformamide / 53 h / 20 °C

2: Et₃N / tetrahydrofuran / 18 h / Heating

With triethylamine; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600720

Reference yield:

: 100-39-0
benzyl bromide

: 929208-88-8
(2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Ag₂O / dimethylformamide / 53 h / 20 °C

2: Et₃N / tetrahydrofuran / 18 h / Heating

With triethylamine; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600720

Reference yield:

: 5336-08-3
D-Ribono-1,4-lactone

: 929208-88-8
(2R,3R,4R)-N-benzyl-5-benzyloxy-2,3-isopropylidenedioxy-4-hydroxypentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / conc. HCl / 18 h / 26 °C

2: 54 percent / Ag₂O / dimethylformamide / 53 h / 20 °C

3: Et₃N / tetrahydrofuran / 18 h / Heating

With hydrogenchloride; triethylamine; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600720