Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

Base Information

Chemical Name:Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide
CAS No.:191938-38-2
Molecular Formula:C₁₆H₁₈N₄O
Molecular Weight:282.345
Hs Code.:

Synonyms:Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

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Chemical Property of Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

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Technology Process of Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

There total 3 articles about Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-36-5
acetyl chloride

: 191938-31-5
C₁₄H₁₆N₄

: 191938-38-2
Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

Guidance literature:: With TEA; In 1,2-dichloro-ethane; for 7h; Ambient temperature;

Reference yield:

: 94843-50-2
N-(4,6-dimethylpyridin-2-yl)benzenecarboxamide

: 191938-38-2
Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: P₄S₁₀ / pyridine / Heating

2: 81 percent / hydrazine hydrate / ethanol / 0.33 h / Ambient temperature

3: 85 percent / TEA / 1,2-dichloro-ethane / 7 h / Ambient temperature

With tetraphosphorus decasulfide; TEA; hydrazine hydrate; In pyridine; ethanol; 1,2-dichloro-ethane;

Reference yield:

: 140869-14-3
N-(4,6-dimethylpyridin-2-yl)benzenethiocarboxamide

: 191938-38-2
Acetic acid [1-(4,6-dimethyl-pyridin-2-ylamino)-1-phenyl-meth-(Z)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / hydrazine hydrate / ethanol / 0.33 h / Ambient temperature

2: 85 percent / TEA / 1,2-dichloro-ethane / 7 h / Ambient temperature

With TEA; hydrazine hydrate; In ethanol; 1,2-dichloro-ethane;