C₂₉H₅₆O₄Si₂

Base Information

Chemical Name:C₂₉H₅₆O₄Si₂
CAS No.:1355616-36-2
Molecular Formula:C₂₉H₅₆O₄Si₂
Molecular Weight:524.932
Hs Code.:

C<sub>29</sub>H<sub>56</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₂₉H₅₆O₄Si₂

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Chemical Property of C₂₉H₅₆O₄Si₂

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Technology Process of C₂₉H₅₆O₄Si₂

There total 8 articles about C₂₉H₅₆O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1355616-35-1
C₂₈H₅₄O₄Si₂

: 333-27-7
methyl trifluoromethanesulfonate

: 1355616-36-2
C₂₉H₅₆O₄Si₂

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ml200254h

Reference yield:

: 1254369-08-8
C₁₆H₂₂O₃

: 1355616-36-2
C₂₉H₅₆O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium osmate; K₃Fe(CN)6; (DHQD)2PHAL; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 36 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 - -45 °C / Inert atmosphere

4.2: 2 h / -78 °C / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -45 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

7.1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 48 h / 20 °C / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; potassium osmate; methanesulfonamide; K₃Fe(CN)6; (DHQD)2PHAL; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Sharpless dihydroxylation;
DOI:10.1021/ml200254h

Reference yield:

: 1355616-33-9
C₂₂H₃₆O₄Si

: 1355616-36-2
C₂₉H₅₆O₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -45 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

3: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 48 h / 20 °C / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml200254h