allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:227601-55-0
Molecular Formula:C₇₉H₈₅NO₁₆
Molecular Weight:1304.54
Hs Code.:

allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Synonyms:allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 8 articles about allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-39-0
benzyl bromide

: 227601-54-9
allyl-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 227601-55-0
allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 227601-43-6
allyl-O-<2,4,6-tri-O-benzyl-β-D-galactopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 227601-55-0
allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Hg(CN)2, HgBr₂, 4 Angstroem molecular sieves / 1.) CH₃CN, 20 deg C, 2 h, 2.) CH₃CN, 20 deg C, 20 h

2: NaBH₄ / tetrahydrofuran; propan-2-ol; H₂O / 12 h / 20 °C

3: 8 h / Heating

4: 96 percent / NaOMe, MeOH / CH₂Cl₂ / 1 h

5: 87 percent / TsOH*H₂O / acetonitrile / 2 h

6: 85 percent / NaH / dimethylformamide / 1 h / 20 °C

With methanol; sodium tetrahydroborate; 4 A molecular sieve; sodium methylate; mercury(II) cyanide; sodium hydride; toluene-4-sulfonic acid; mercury dibromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 227601-55-0
allyl-O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Hg(CN)2, HgBr₂, 4 Angstroem molecular sieves / 1.) CH₃CN, 20 deg C, 2 h, 2.) CH₃CN, 20 deg C, 20 h

2: NaBH₄ / tetrahydrofuran; propan-2-ol; H₂O / 12 h / 20 °C

3: 8 h / Heating

4: 96 percent / NaOMe, MeOH / CH₂Cl₂ / 1 h

5: 87 percent / TsOH*H₂O / acetonitrile / 2 h

6: 85 percent / NaH / dimethylformamide / 1 h / 20 °C

With methanol; sodium tetrahydroborate; 4 A molecular sieve; sodium methylate; mercury(II) cyanide; sodium hydride; toluene-4-sulfonic acid; mercury dibromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;