N-cyclohexyl-N-tosylpropiolamide

Base Information

Chemical Name:N-cyclohexyl-N-tosylpropiolamide
CAS No.:1309932-50-0
Molecular Formula:C₁₆H₁₉NO₃S
Molecular Weight:305.398
Hs Code.:

Synonyms:N-cyclohexyl-N-tosylpropiolamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-N-tosylpropiolamide

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Technology Process of N-cyclohexyl-N-tosylpropiolamide

There total 1 articles about N-cyclohexyl-N-tosylpropiolamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: propynoyl pivaloyl anhydride

: 80-30-8
N-cyclohexyl-p-toluenesulfonamide

: 1309932-50-0
N-cyclohexyl-N-tosylpropiolamide

Guidance literature:: N-cyclohexyl-p-toluenesulfonamide; With n-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h; Inert atmosphere;

propynoyl pivaloyl anhydride; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃;
DOI:10.1021/jacs.0c02052

Reference yield: 58.0%

: 1309932-50-0
N-cyclohexyl-N-tosylpropiolamide

: 1309932-61-3
(E)-N-cyclohexyl-3-(N-cyclohexyl-4-methylphenylsulfonamido)-N-tosylpropenamide

Guidance literature:: With triethylamine; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1259561

Reference yield: 48.0%

: 1309932-50-0
N-cyclohexyl-N-tosylpropiolamide

: 1489-69-6
Cyclopropanecarboxaldehyde

: (±)-(4R,5R)-2-cyclohexyl-5-(cyclopropanecarbonyl)-4-(p-tolyl)isothiazolidin-3-one 1,1-dioxide

Guidance literature:: With eosin Y disodium salt; In acetonitrile; at 80 ℃; for 48h; diastereoselective reaction; Schlenk technique; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/jacs.0c02052