9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

Base Information

Chemical Name:9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol
CAS No.:1353007-15-4
Molecular Formula:C₃₅H₄₆F₇NO₃S
Molecular Weight:693.81
Hs Code.:

Synonyms:9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

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Chemical Property of 9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

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Technology Process of 9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

There total 6 articles about 9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353008-58-8
9-(6-bromohexyl)-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

: 1353009-20-7
N-tert-butyl-3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propan-1-amine

: 1353007-15-4
9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

Guidance literature:: With sodium carbonate; sodium iodide; In acetonitrile;

Reference yield:

: 199730-54-6
3-chloropropyl 4,4,5,5,5-pentafluoropentyl sulphone

: 1353007-15-4
9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; water / 72 h / 75 °C

2: sodium iodide; sodium carbonate / acetonitrile

With sodium carbonate; sodium iodide; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 209325-64-4
4,4,5,5,5-pentafluoropentyl-4-methylbenzene sulphonate

: 1353007-15-4
9-[6-(tert-butyl{3-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]propyl}amino)hexyl]-4-fluoro-8-(4-fluorophenyl)-6,7-dihydro-5H-benzo[7]annulen-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: potassium thioacetate / acetone / Reflux

2: sodium methylate / methanol / 0.5 h / 20 °C / Cooling with ice

3: 3-chloro-benzenecarboperoxoic acid / chloroform / 10 - 20 °C / Cooling with ice

4: N,N-dimethyl-formamide; water / 72 h / 75 °C

5: sodium iodide; sodium carbonate / acetonitrile

With sodium methylate; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; potassium thioacetate; In methanol; chloroform; water; N,N-dimethyl-formamide; acetone; acetonitrile;