[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

Base Information

Chemical Name:[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde
CAS No.:1267606-24-5
Molecular Formula:C₃₁H₄₇NO₂
Molecular Weight:465.72
Hs Code.:

Synonyms:[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

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Chemical Property of [2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

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Technology Process of [2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

There total 5 articles about [2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.8%

: 1267606-21-2
[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetonitrile

: 1267606-24-5
[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

Guidance literature:: [2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetonitrile; With diisobutylaluminium hydride; In toluene; at 0 ℃; for 1.5h; Cooling with acetone-dry ice; Inert atmosphere;

With ammonium chloride; In toluene; at 0 ℃;

Reference yield:

: 35493-25-5
2-butyl-3,5,5-trimethyl-2-cyclohexenone

: 1267606-24-5
[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol; ammonium acetate; sodium / 22 h / 60 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / Inert atmosphere; Cooling with acetone-dry ice

2.2: 0.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

3.1: diisobutylaluminium hydride / toluene / 1.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

3.2: 0 °C

With ethanol; ammonium acetate; sodium; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; toluene;

Reference yield:

: 1267606-20-1
3-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]-2-butyl-5,5-dimethyl-2-cyclohexenone

: 1267606-24-5
[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / Inert atmosphere; Cooling with acetone-dry ice

1.2: 0.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 1.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

2.2: 0 °C

With diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; toluene;