2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Base Information

Chemical Name:2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile
CAS No.:1267606-25-6
Molecular Formula:C₄₇H₅₃F₃N₄O₂
Molecular Weight:762.959
Hs Code.:

2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Synonyms:2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

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Chemical Property of 2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

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Technology Process of 2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

There total 6 articles about 2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.9%

: 1267606-24-5
[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetaldehyde

: 436097-14-2
[3-cyano-4-methyl-5-phenyl-5-(trifluoromethyl)-2(5H)-furanylidene]propanedinitrile

: 1267606-25-6
2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Guidance literature:: at 50 ℃; for 0.666667h;

Reference yield:

: 35493-25-5
2-butyl-3,5,5-trimethyl-2-cyclohexenone

: 1267606-25-6
2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol; ammonium acetate; sodium / 22 h / 60 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / Inert atmosphere; Cooling with acetone-dry ice

2.2: 0.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

3.1: diisobutylaluminium hydride / toluene / 1.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

3.2: 0 °C

4.1: 0.67 h / 50 °C

With ethanol; ammonium acetate; sodium; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; toluene;

Reference yield:

: 1267606-21-2
[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]acetonitrile

: 1267606-25-6
2-[4-[3-[2-butyl-3-[2-(4-dibutylamino-2-methoxyphenyl) vinyl]-5,5-dimethyl-2-cyclohexenylidene]-1-propenyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride / toluene / 1.5 h / 0 °C / Cooling with acetone-dry ice; Inert atmosphere

1.2: 0 °C

2.1: 0.67 h / 50 °C

With diisobutylaluminium hydride; In toluene;