tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate
CAS No.:1402840-87-2
Molecular Formula:C₃₁H₂₈ClN₃O₅
Molecular Weight:558.033
Hs Code.:

Synonyms:tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

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Chemical Property of tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

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Technology Process of tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

There total 3 articles about tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53716-49-7,52263-83-9
2-(6-chloro-carbazol-2-yl)-propionic acid

: 1402840-87-2
tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 3 h / 20 °C

2.1: dmap; triethylamine / acetonitrile / 2 h / 20 °C

With dmap; potassium carbonate; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm3011146

Reference yield:

: 1-tert-butoxycarbonyl-1H-imidazole-4-carboxylic acid

: 1402840-87-2
tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

2: dmap; triethylamine / acetonitrile / 2 h / 20 °C

With dmap; oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm3011146

Reference yield:

: 100-39-0
benzyl bromide

: 1402840-87-2
tert-butyl 4-(2-(1-(benzyloxy)-1-oxoprop-2-yl)-6-chloro-9H-carbazol-9-ylcarbonyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 3 h / 20 °C

2.1: dmap; triethylamine / acetonitrile / 2 h / 20 °C

With dmap; potassium carbonate; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm3011146