(5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

Base Information

• Chemical Name: (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one
• CAS No.: 625437-69-6
• Molecular Formula: C₂₁H₃₃NO₂Si
• Molecular Weight: 359.584

Synonyms:(5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

Chemical Property of (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

Chemical Property:

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Technology Process of (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

There total 10 articles about (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyltributylstanane (24850-33-7) + 6-benzenesulfonyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one → (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one (625437-69-6) + (5S,6R)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

Guidance literature:

With zinc(II) chloride; In dichloromethane; at -78 - 20 ℃;

DOI:10.1055/s-2003-40988

Reference yield:

allyl-trimethyl-silane (762-72-1) + 1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-6-methoxy-piperidin-2-one (625437-76-5) → (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one (625437-69-6) + (5S,6R)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃;

DOI:10.1055/s-2003-40988

Reference yield:

allyl-trimethyl-silane (762-72-1) + acetic acid 1-benzyl-3-(tert-butyl-dimethyl-silanyloxy)-6-oxo-piperidin-2-yl ester (625437-77-6) → (5S,6S)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one (625437-69-6) + (5S,6R)-6-Allyl-1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-piperidin-2-one

Guidance literature:

With titanium tetrachloride; In dichloromethane; at -78 - 20 ℃;

DOI:10.1055/s-2003-40988

upstream raw materials:

allyltributylstanane

allyl-trimethyl-silane

1-benzyl-5-(tert-butyl-dimethyl-silanyloxy)-6-methoxy-piperidin-2-one

acetic acid 1-benzyl-3-(tert-butyl-dimethyl-silanyloxy)-6-oxo-piperidin-2-yl ester

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