(4Z,6E)-(2S,3S,8S,9S)-3-tert-Butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-10-phenyl-deca-4,6-dienoic acid methyl ester

Base Information

Chemical Name:(4Z,6E)-(2S,3S,8S,9S)-3-tert-Butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-10-phenyl-deca-4,6-dienoic acid methyl ester
CAS No.:134440-91-8
Molecular Formula:C₂₆H₃₉NO₅
Molecular Weight:445.599
Hs Code.:

Synonyms:(4Z,6E)-(2S,3S,8S,9S)-3-tert-Butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-10-phenyl-deca-4,6-dienoic acid methyl ester

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Chemical Property of (4Z,6E)-(2S,3S,8S,9S)-3-tert-Butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-10-phenyl-deca-4,6-dienoic acid methyl ester

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Technology Process of (4Z,6E)-(2S,3S,8S,9S)-3-tert-Butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-10-phenyl-deca-4,6-dienoic acid methyl ester

There total 57 articles about (4Z,6E)-(2S,3S,8S,9S)-3-tert-Butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-10-phenyl-deca-4,6-dienoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 180133-64-6
(2S,3R,4E)-3-(tert-butoxycarbonyl)amino-2-methyl-5-iodo-4-pentenoic acid methyl ester

: C₁₄H₂₁BO₃

: 134440-91-8
(2S,3S,8S,9S,4E,6E)-3-(tert-butoxycarbonyl)amino-9-methoxy-2,6,8-trimethyl-10-phenyl-4,6-decadienoic acid methyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide; In tetrahydrofuran; water; at 0 ℃; for 2h;
DOI:10.1021/ja961683e

Reference yield: 58.0%

: 180133-63-5
(4S,5S,2E)-2-iodo-5-methoxy-4-methyl-6-phenyl-2-hexene

: (E)-(2S,3R)-3-tert-Butoxycarbonylamino-2-methyl-5-trimethylstannanyl-pent-4-enoic acid methyl ester

: 134440-91-8
(2S,3S,8S,9S,4E,6E)-3-(tert-butoxycarbonyl)amino-9-methoxy-2,6,8-trimethyl-10-phenyl-4,6-decadienoic acid methyl ester

: 134440-91-8
(2S,3S,8S,9S,4E,6Z)-3-(tert-butoxycarbonyl)amino-9-methoxy-2,6,8-trimethyl-10-phenyl-4,6-decadienoic acid methyl ester

Guidance literature:: dichloro bis(acetonitrile) palladium(II); In N,N-dimethyl-formamide; for 4h; Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4020(96)01056-3

Reference yield: 58.0%

: 180133-63-5
(4S,5S,2E)-2-iodo-5-methoxy-4-methyl-6-phenyl-2-hexene

: (E)-(2S,3R)-3-tert-Butoxycarbonylamino-2-methyl-5-trimethylstannanyl-pent-4-enoic acid methyl ester

: 134440-91-8
(2S,3S,8S,9S,4E,6E)-3-(tert-butoxycarbonyl)amino-9-methoxy-2,6,8-trimethyl-10-phenyl-4,6-decadienoic acid methyl ester

: 134440-91-8
(2S,3S,8S,9S,4E,6Z)-3-(tert-butoxycarbonyl)amino-9-methoxy-2,6,8-trimethyl-10-phenyl-4,6-decadienoic acid methyl ester

Guidance literature:: dichloro bis(acetonitrile) palladium(II); In N,N-dimethyl-formamide; for 4h; Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4020(96)01056-3