[PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C₆H₆

Base Information

• Chemical Name: [PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C₆H₆
• CAS No.: 891753-17-6
• Molecular Formula: C₆H₆*C₃₉H₃₉ClNOPdSb
• Molecular Weight: 879.481

Synonyms:[PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C₆H₆

Chemical Property of [PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C₆H₆

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Technology Process of [PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C₆H₆

There total 1 articles about [PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C₆H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

(+/-)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane (891191-65-4,891191-58-5,891191-64-3) + (S)-(+)-di-μ-chloro-bis[1-[(dimethylamino)ethyl]-2-naphthyl-C,N]dipalladium(II) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → [PdCl(Sb(S)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))] + [PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C6H6 (891753-17-6)

Guidance literature:

In dichloromethane; (Ar); Pd complex was added to stirred soln. of Sb compd. in CH2Cl2 at room temp.; mixt. was stirred for 10 min; concd. (vac.); septd. (silica gel, CH2Cl2/hexane, 10/1); recrystd. (C6H6/ether); elem. anal.;

DOI:10.1016/j.jorganchem.2005.10.042

Reference yield: 95.0%

[PdCl(Sb(R)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane)((S)-2-(1-(dimethylamino)ethyl)naphthyl))]*C6H6 (891753-17-6) → Sb(S)-(+)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane (891191-58-5,891191-64-3,891191-65-4)

Guidance literature:

With Ph₃P; In dichloromethane; (Ar); P compd. (1.1 equiv.) was added to soln. of Pd complex in CH2Cl2 at room temp.; mixt. was stirred for 10 min; concd. (vac.); chromd. (silica gel, hexane/CH2Cl2, 4/1);

DOI:10.1016/j.jorganchem.2005.10.042

upstream raw materials:

(+/-)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane

benzene

Downstream raw materials:

Sb(S)-(+)-(2-methoxymethylphenyl)(1-naphthyl)(4-tolyl)stibane

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