(S)-(-)-2, 2 DIMETHYL-1,3-DIOXOLANE-4-CARBOXYLATE

Base Information

• Chemical Name: (S)-(-)-2, 2 DIMETHYL-1,3-DIOXOLANE-4-CARBOXYLATE
• CAS No.: 117205-81-9
• Molecular Formula: C6H10 O4 . K
• Molecular Weight: 0
• Hs Code.: 2932999099
• Mol file: 117205-81-9.mol

Synonyms:1,3-Dioxolane-4-carboxylicacid, 2,2-dimethyl-, potassium salt, (4S)- (9CI); 1,3-Dioxolane-4-carboxylicacid, 2,2-dimethyl-, potassium salt, (S)-;(4S)-2,2-Dimethyl-1,3-dioxolane-4-carboxylic acid potassium salt

Chemical Property of (S)-(-)-2, 2 DIMETHYL-1,3-DIOXOLANE-4-CARBOXYLATE

Chemical Property:

• PSA: 58.59000
• LogP: -1.11220

Purity/Quality:

(4S)-2,2-Dimethyl-1,3-dioxolane-4-carboxylicAcidPotassiumSalt ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (4S)-2,2-Dimethyl-1,3-dioxolane-4-carboxylic Acid Potassium Salt is a intermediate in the synthesis of methoxypropionamide derivatives with anticonvulsant activities (4S)-2,2-Dimethyl-1,3-dioxolane-4-carboxylic Acid Potassium Salt is an intermediate in the synthesis of methoxypropionamide derivatives with anticonvulsant activities

Technology Process of (S)-(-)-2, 2 DIMETHYL-1,3-DIOXOLANE-4-CARBOXYLATE

There total 4 articles about (S)-(-)-2, 2 DIMETHYL-1,3-DIOXOLANE-4-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

5,6-O-isopropylidene-L-ascorbic acid (15042-01-0,15042-06-5,50271-42-6,64550-45-4,127514-13-0) → potassium (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (117205-81-9)

Guidance literature:

With potassium hydroxide; at 20 ℃; for 18h; nickel(III) oxide hydroxide, 0.15 A;

DOI:10.1055/s-1988-27462

Reference yield:

methyl (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (60456-21-5) → potassium (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (117205-81-9)

Guidance literature:

With potassium permanganate; In methanol; at 50 ℃; for 2h;

Reference yield:

(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde (22323-80-4) → potassium (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (117205-81-9)

Guidance literature:

With potassium hydroxide; potassium permanganate; In water; at 0 ℃; Yield given;

DOI:10.1021/jo9601472

upstream raw materials:

5,6-O-isopropylidene-L-ascorbic acid

(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

1,2:5,6-di-O-isopropylidene-D-mannitol

methyl (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Downstream raw materials:

2,3-O-isopropylidene-L-glyceric acid

(2S)-2,3-isopropylideneglyceryl chloride

N-(O-Isopropyliden-D-glyceroyl)-L-phenylalanin

N-(O-Isopropyliden-D-glyceroyl)-L-phenylalaninmethylester

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