2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine

Base Information

• Chemical Name: 2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine
• CAS No.: 912806-66-7
• Molecular Formula: C₁₂H₂₂Cl₂N₂P₂
• Molecular Weight: 327.174
• Mol file: 912806-66-7.mol

Synonyms:2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine

Chemical Property of 2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine

There total 2 articles about 2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

cyclohexylamine (108-91-8,157973-60-9) → 2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine (912806-66-7)

Guidance literature:

cyclohexylamine; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 1h;

With phosphorus trichloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 50h;

DOI:10.1039/b607332h

Reference yield: 9.5%

cyclohexylamine (108-91-8,157973-60-9) → 2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine (912806-66-7) + C6H11Cl4NP2

Guidance literature:

With triethylamine; phosphorus trichloride; In toluene; at -78 - 20 ℃; for 8h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1021/jacs.1c07042

Reference yield: 61.0%

2,4-dichloro-1,3-dicyclohexyl-[1,3,2,4]diazadiphosphetidine (912806-66-7) + 3,3’-dimethyl-[1,1’-binaphthalene]-2,2’-diol (39648-71-0,55442-34-7,55515-98-5,55515-99-6) → C34H38N2O2P2

Guidance literature:

With triethylamine; In toluene; at 110 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.1c07042

upstream raw materials:

cyclohexylamine