2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

Base Information

Chemical Name:2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol
CAS No.:129929-71-1
Molecular Formula:C₂₂H₃₀O₆
Molecular Weight:390.477
Hs Code.:

Synonyms:2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

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Chemical Property of 2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

Chemical Property:

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Technology Process of 2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

There total 8 articles about 2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: methyl 2-(2-formyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzoate

: 129929-71-1
2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; 1) 0 deg C, 15 min, 2) r.t., 1 h;
DOI:10.1039/P19900001371

Reference yield:

: 129929-80-2
2-hydroxy-6-isopropoxybenzaldehyde

: 129929-71-1
2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / potassium carbonate / diethyl ether / 35 h

2: 68 percent / toluene p-sulphonic acid / benzene / 1 h / Heating

3: 73 percent / lithium aluminium hydride / tetrahydrofuran / 1 h / 0 °C

4: 26 percent / pyridine, potassium carbonate / CuO / 24 h / Heating

5: 93 percent / lithium aluminium hydride / diethyl ether / 1) 0 deg C, 15 min, 2) r.t., 1 h

With pyridine; lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; copper(II) oxide; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1039/P19900001371

Reference yield:

: 129929-66-4
2-hydroxy-6-isopropoxybenzyl alcohol

: 129929-71-1
2-(2-hydroxymethyl-3-isopropoxyphenoxy)-3-isopropoxy-5-methoxy-4-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / manganese dioxide / diethyl ether / 30 h / Ambient temperature

2: 71 percent / potassium carbonate / diethyl ether / 35 h

3: 68 percent / toluene p-sulphonic acid / benzene / 1 h / Heating

4: 73 percent / lithium aluminium hydride / tetrahydrofuran / 1 h / 0 °C

5: 26 percent / pyridine, potassium carbonate / CuO / 24 h / Heating

6: 93 percent / lithium aluminium hydride / diethyl ether / 1) 0 deg C, 15 min, 2) r.t., 1 h

With pyridine; manganese(IV) oxide; lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; copper(II) oxide; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1039/P19900001371