Methyl 2-methylbenzhydrylamine

Base Information

Chemical Name:Methyl 2-methylbenzhydrylamine
CAS No.:42882-30-4
Molecular Formula:C₁₅H₁₇N
Molecular Weight:211.307
Hs Code.:
Nikkaji Number:J2.475.345J

Synonyms:Methyl 2-methylbenzhydrylamine;AKOS008962044;Methyl [(2-methylphenyl)(phenyl)methyl]amine

Suppliers and Price of Methyl 2-methylbenzhydrylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-methylbenzhydrylamine

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:211.136099547
Heavy Atom Count:16
Complexity:196

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=CC=C1C(C2=CC=CC=C2)NC

Technology Process of Methyl 2-methylbenzhydrylamine

There total 4 articles about Methyl 2-methylbenzhydrylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (+/-)-1,3-dimethyl-3-nitroso-1-(phenyl-o-tolyl-methyl)urea

: 42882-30-4
(+/-)-N-methyl-1-phenyl-1-o-tolylmethanamine

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 80 ℃;
DOI:10.1021/ja071523a

Reference yield:

: 944338-89-0
(+/-)-1,3-dimethyl-1-(phenyl-o-tolyl-methyl)urea

: 42882-30-4
(+/-)-N-methyl-1-phenyl-1-o-tolylmethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / t-BuONO / CH₂Cl₂ / 24 h / 20 °C

2: 80 percent / LiOH / tetrahydrofuran; H₂O / 80 °C

With lithium hydroxide; tert.-butylnitrite; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja071523a

Reference yield:

: 944338-76-5
1-benzyl-1,3-dimethyl-3-o-tolylurea

: 42882-30-4
(+/-)-N-methyl-1-phenyl-1-o-tolylmethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / s-BuLi / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C

2: 90 percent / t-BuONO / CH₂Cl₂ / 24 h / 20 °C

3: 80 percent / LiOH / tetrahydrofuran; H₂O / 80 °C

With lithium hydroxide; tert.-butylnitrite; sec.-butyllithium; In tetrahydrofuran; dichloromethane; cyclohexane; water;
DOI:10.1021/ja071523a