α-bromo-2,6-diisopropylstyrene

Base Information

Chemical Name:α-bromo-2,6-diisopropylstyrene
CAS No.:156023-28-8
Molecular Formula:C₁₄H₁₉Br
Molecular Weight:267.209
Hs Code.:

Synonyms:α-bromo-2,6-diisopropylstyrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-bromo-2,6-diisopropylstyrene

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Technology Process of α-bromo-2,6-diisopropylstyrene

There total 7 articles about α-bromo-2,6-diisopropylstyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2,6-diisopropylacetophenone hydrazone

: 156023-28-8
α-bromo-2,6-diisopropylstyrene

Guidance literature:: With pyridine; bromine; In chloroform; 1.) r.t., 2.5 h, 2.) r.t. to 35 deg C;

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 156023-28-8
α-bromo-2,6-diisopropylstyrene

Guidance literature:: Multi-step reaction with 7 steps

1: BrCCl₃, isopentyl nitrite / 1,2-dimethoxy-ethane / 14 h / 75 °C

2: 1.) Mg, iodine, 1,2-dibromoethane / 1.) ether, reflux, 15 h, 2.) ether, reflux, 2 h

3: 48 percent / KHSO₄ / 180 °C / 40 Torr

4: 72 percent / Br₂ / CHCl₃ / 0.08 h

5: 32 percent / KOH / ethanol / 0.17 h / 50 °C

6: 30percent NaNH₂ / toluene; tetrahydrofuran / 10 h / Heating

7: 47percent HBr, NaBr / acetic acid / 0.5 h

With potassium hydroxide; potassium hydrogensulfate; Bromotrichloromethane; hydrogen bromide; bromine; iodine; sodium amide; magnesium; ethylene dibromide; sodium bromide; isopentyl nitrite; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; chloroform; acetic acid; toluene;

Reference yield:

: 57190-17-7
2-bromo-1,3-diisopropylbenzene

: 156023-28-8
α-bromo-2,6-diisopropylstyrene

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Mg, iodine, 1,2-dibromoethane / 1.) ether, reflux, 15 h, 2.) ether, reflux, 2 h

2: 48 percent / KHSO₄ / 180 °C / 40 Torr

3: 72 percent / Br₂ / CHCl₃ / 0.08 h

4: 32 percent / KOH / ethanol / 0.17 h / 50 °C

5: 30percent NaNH₂ / toluene; tetrahydrofuran / 10 h / Heating

6: 47percent HBr, NaBr / acetic acid / 0.5 h

With potassium hydroxide; potassium hydrogensulfate; hydrogen bromide; bromine; iodine; sodium amide; magnesium; ethylene dibromide; sodium bromide; In tetrahydrofuran; ethanol; chloroform; acetic acid; toluene;