Technology Process of 2-(3-Brom-4-methoxyphenyl)-1H-pyrrol
There total 6 articles about 2-(3-Brom-4-methoxyphenyl)-1H-pyrrol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ethanol; ammonia;
for 4h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 1 h / Heating
2: 1.) Mg / 1.) THF, 30 min, reflux; 2.) THF, 12 h, room temperature
3: glacial acetic acid, conc. HCl / H2O / 72 h / Ambient temperature
4: glacial acetic acid, conc. HCl / H2O / 72 h / Ambient temperature
5: 43 percent / 15 percent NH3/ethanol / 4 h / Ambient temperature
With
hydrogenchloride; thionyl chloride; ethanol; ammonia; magnesium; acetic acid;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 77 percent / KOH / methanol; H2O / 4 h / Heating
2: thionyl chloride / 1 h / Heating
3: 1.) Mg / 1.) THF, 30 min, reflux; 2.) THF, 12 h, room temperature
4: glacial acetic acid, conc. HCl / H2O / 72 h / Ambient temperature
5: glacial acetic acid, conc. HCl / H2O / 72 h / Ambient temperature
6: 43 percent / 15 percent NH3/ethanol / 4 h / Ambient temperature
With
hydrogenchloride; potassium hydroxide; thionyl chloride; ethanol; ammonia; magnesium; acetic acid;
In
methanol; water;
