7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate

Base Information

• Chemical Name: 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate
• CAS No.: 76017-77-1
• Molecular Formula: CF₃O₃S*C₃₄H₂₈N
• Molecular Weight: 599.673

Synonyms:7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate

Chemical Property of 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate

There total 5 articles about 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5,6,8,9-tetrahydro-7-phenyldibenzoxanthyilium triflouromethanesulphonate (73377-38-5) + p-toluidine (106-49-0,12221-03-3) → 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate (76017-77-1)

Guidance literature:

In methanol; at 85 ℃; for 12h; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.202000412

Reference yield:

benzaldehyde (100-52-7) → 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate (76017-77-1)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: tetrahydrofuran / 12 h / 0 - 85 °C / Schlenk technique; Inert atmosphere

3: methanol / 12 h / 85 °C / Schlenk technique; Inert atmosphere

With sodium hydroxide; In tetrahydrofuran; methanol; water;

DOI:10.1002/chem.202000412

Reference yield:

3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 7-phenyl-14-(p-tolyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridin-14-ium trifluoromethanesulfonate (76017-77-1)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: tetrahydrofuran / 12 h / 0 - 85 °C / Schlenk technique; Inert atmosphere

3: methanol / 12 h / 85 °C / Schlenk technique; Inert atmosphere

With sodium hydroxide; In tetrahydrofuran; methanol; water;

DOI:10.1002/chem.202000412

upstream raw materials:

5,6,8,9-tetrahydro-7-phenyldibenzoxanthyilium triflouromethanesulphonate

p-toluidine

2-benzylidene-1-tetralone

3,4-dihydronaphthalene-1(2H)-one

Downstream raw materials:

1-(2,2-diphenylethyl)-4-methylbenzene

p-tolylboronic pinacol ester

4-(1'-methyl-1'-nitroethyl)toluene

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