C₂₂H₂₈N₄O₅S

Base Information

Chemical Name:C₂₂H₂₈N₄O₅S
CAS No.:1355249-47-6
Molecular Formula:C₂₂H₂₈N₄O₅S
Molecular Weight:460.554
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>4</sub>O<sub>5</sub>S

Synonyms:C₂₂H₂₈N₄O₅S

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Chemical Property of C₂₂H₂₈N₄O₅S

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Technology Process of C₂₂H₂₈N₄O₅S

There total 6 articles about C₂₂H₂₈N₄O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1355249-46-5
C₂₄H₂₈N₄O₆S

: 1355249-47-6
C₂₂H₂₈N₄O₅S

Guidance literature:: C₂₄H₂₈N₄O₆S; With lithium borohydride; In tetrahydrofuran; for 2h; Reflux;

With water; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 944805-17-8
tert-butyl (4-bromo-5-formylthiazol-2-yl)carbamate

: 1355249-47-6
C₂₂H₂₈N₄O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 2.33 h / -78 - 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 16 h / 20 °C

3.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 1.5 h / 80 °C / Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / 2 h / Reflux

4.2: 20 °C

With potassium phosphate; lithium borohydride; pyridinium chlorochromate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1355249-29-4
ethyl 4-iodo-1-(4-methoxybenzyl)-1H-pyrazole-3-carboxylate

: 1355249-47-6
C₂₂H₂₈N₄O₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C

2.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 1.5 h / 80 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 2 h / Reflux

3.2: 20 °C

With potassium phosphate; lithium borohydride; n-butyllithium; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; water; N,N-dimethyl-formamide;