allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside
CAS No.:1349065-21-9
Molecular Formula:C₂₆H₃₁ClO₇
Molecular Weight:490.981
Hs Code.:

Synonyms:allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

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Technology Process of allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

There total 6 articles about allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 144174-52-7
allyl 4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

: 79-04-9
chloroacetyl chloride

: 1349065-21-9
allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h; Cooling with ice; Inert atmosphere;

Reference yield:

: 89821-78-3
allyl 4-O-benzyl-α-L-rhamnopyranoside

: 1349065-21-9
allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / toluene / 3 h / Reflux

1.2: 2 h / Reflux

2.1: pyridine / dichloromethane / 3 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; di(n-butyl)tin oxide; In dichloromethane; toluene;

Reference yield:

: C₁₉H₂₆O₅

: 1349065-21-9
allyl 4-O-benzyl-2-O-chloroacetyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / water / 3 h / 60 °C

2.1: di(n-butyl)tin oxide / toluene / 3 h / Reflux

2.2: 2 h / Reflux

3.1: pyridine / dichloromethane / 3 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; di(n-butyl)tin oxide; acetic acid; In dichloromethane; water; toluene;