2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester

Base Information

• Chemical Name: 2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester
• CAS No.: 124787-28-6
• Molecular Formula: C₁₆H₂₄O₃
• Molecular Weight: 264.365
• Mol file: 124787-28-6.mol

Synonyms:2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester

Chemical Property of 2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester

There total 1 articles about 2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid (63965-90-2) + (2-methylcyclopent-1-enyl)methanol (81328-62-3) → 2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester (124787-28-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In diethyl ether;

DOI:10.1016/S0040-4039(01)80687-0

Reference yield:

2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid 2-methyl-cyclopent-1-enylmethyl ester (124787-28-6) + tert-butyldimethylsilyl chloride (18162-48-6) → C22H38O3Si + C22H38O3Si

Guidance literature:

With potassium hexamethylsilazane; 18-crown-6 ether; Multistep reaction. Title compound not separated from byproducts; 1.) -78 deg C, THF, 2.) -100 deg C, HMPA; 65 deg C;

DOI:10.1016/S0040-4039(01)80687-0

upstream raw materials:

2-Methoxy-4-methyl-cyclohex-2-enecarboxylic acid

(2-methylcyclopent-1-enyl)methanol