Technology Process of 4-aminophenyl benzyl sulfoxide
There total 6 articles about 4-aminophenyl benzyl sulfoxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; bis(η3-allyl-μ-chloropalladium(II)); cesium fluoride;
In
2-methyltetrahydrofuran;
at 110 ℃;
for 24h;
chemoselective reaction;
Inert atmosphere;
Glovebox;
Sealed tube;
DOI:10.1021/jacs.5b08117
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,2'-azobis(isobutyronitrile) / neat (no solvent) / Inert atmosphere
2: sodium periodate / methanol; water / Inert atmosphere
3: bis(η3-allyl-μ-chloropalladium(II)); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; cesium fluoride / 2-methyltetrahydrofuran / 24 h / 110 °C / Inert atmosphere; Glovebox; Sealed tube
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium periodate; bis(η3-allyl-μ-chloropalladium(II)); 2,2'-azobis(isobutyronitrile); cesium fluoride;
In
2-methyltetrahydrofuran; methanol; water;
DOI:10.1021/jacs.5b08117
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium periodate / methanol; water / Inert atmosphere
2: bis(η3-allyl-μ-chloropalladium(II)); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; cesium fluoride / 2-methyltetrahydrofuran / 24 h / 110 °C / Inert atmosphere; Glovebox; Sealed tube
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium periodate; bis(η3-allyl-μ-chloropalladium(II)); cesium fluoride;
In
2-methyltetrahydrofuran; methanol; water;
DOI:10.1021/jacs.5b08117
