5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

Base Information

Chemical Name:5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol
CAS No.:118668-49-8
Molecular Formula:C₂₀H₃₄O₃S
Molecular Weight:354.554
Hs Code.:

Synonyms:5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

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Chemical Property of 5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

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Technology Process of 5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

There total 3 articles about 5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118217-76-8
1,3-Dibromo-2-tert-butylsulfanyl-propane

: 118668-49-8
5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: MCPBA / CCl₄; CH₂Cl₂ / -20 deg C, 15 min, then room t., 3 h

2: 80 percent / NaOAc / tetrahydrofuran / 2.5 h / Ambient temperature; in ultrasound laboratory cleaner

3: 1.) Zn foil, 1,2-dibromoethane / 1.) THF, heating to start boiling, then 30-35 deg C, 15-20 min, 2.) THF, 45-52 deg C

With sodium acetate; ethylene dibromide; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1016/S0040-4020(01)86151-2

Reference yield:

: 118668-51-2
1,3-dibromo-2-(tert-butylsulfonyl)-propane

: 118668-49-8
5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaOAc / tetrahydrofuran / 2.5 h / Ambient temperature; in ultrasound laboratory cleaner

2: 1.) Zn foil, 1,2-dibromoethane / 1.) THF, heating to start boiling, then 30-35 deg C, 15-20 min, 2.) THF, 45-52 deg C

With sodium acetate; ethylene dibromide; zinc; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)86151-2

Reference yield:

: 79-77-6,14901-07-6
(E)-β-ionone

: 97147-24-5
2-(tert-butylsulfonyl)-2-propenyl bromide

: 118668-49-8
5-tert-butylsulfonyl-3-methyl-1-(2,6,6-trimethyl-1-cyclohexenyl)1,5 hexadien-3-ol

Guidance literature:: With ethylene dibromide; zinc; Yield given. Multistep reaction; 1.) THF, heating to start boiling, then 30-35 deg C, 15-20 min, 2.) THF, 45-52 deg C;
DOI:10.1016/S0040-4020(01)86151-2