ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Base Information

Chemical Name:ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside
CAS No.:86646-60-8
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

Synonyms:ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Suppliers and Price of ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

There total 3 articles about ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 100-39-0
benzyl bromide

: 86646-59-5
ethyl 2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talo-pyranoside

: 86646-60-8
ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Guidance literature:: With sodium hydride; In 1,2-dimethoxyethane; for 4h; Ambient temperature;
DOI:10.1021/ja00356a026

Reference yield:

: 25474-16-2
(2R)-2r-acetoxymethyl-6t-ethoxy-6H-pyran-3-one

: 86646-60-8
ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / AlCl₃ / CH₂Cl₂ / 2.5 h / -78 - -40 °C

2: 80 percent / LiAlH₄

3: Ambient temperature

With lithium aluminium tetrahydride; aluminium trichloride; In dichloromethane;
DOI:10.1039/c39800000006

Reference yield:

: 74198-08-6
ethyl 6-O-acetyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-lyxohexopyranosid-4-ulose

: 86646-60-8
ethyl 6-O-benzyl-2,3-C-(2-butene-1,4-diyl)-2,3-dideoxy-α-D-talopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / LiAlH₄

2: Ambient temperature

With lithium aluminium tetrahydride;
DOI:10.1039/c39800000006