3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

Base Information

Chemical Name:3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone
CAS No.:244262-42-8
Molecular Formula:C₃₉H₃₆N₂O₁₅
Molecular Weight:772.719
Hs Code.:

Synonyms:3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

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Chemical Property of 3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

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Technology Process of 3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

There total 3 articles about 3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₃₉H₃₈N₂O₁₅

: 244262-42-8
3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

Guidance literature:: With chromium(VI) oxide; at 0 ℃; for 3h;
DOI:10.1021/jo990177f

Reference yield:

: 207743-22-4
4,4'-dimethoxy-3,3'-dimethoxycarbonyl-5,5'-dinitrobenzophenone

: 244262-42-8
3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / Zn dust; AcOH / 1 h / 45 °C

2: pyridine / CH₂Cl₂

3: 85 percent / CrO₃ / 3 h / 0 °C

With pyridine; chromium(VI) oxide; acetic acid; zinc; In dichloromethane; 1: Reduction / 2: Acylation / 3: Oxidation;
DOI:10.1021/jo990177f

Reference yield:

: 244262-39-3
1,1'-bis(3-amino-4-methoxy-5-methoxycarbonylphenyl)methanol

: 244262-42-8
3,3'-bis(4-methoxy-3-methoxycarbonylbenzamido)-4,4'-dimethoxy-5,5'-dimethoxycarbonylbenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂

2: 85 percent / CrO₃ / 3 h / 0 °C

With pyridine; chromium(VI) oxide; In dichloromethane; 1: Acylation / 2: Oxidation;
DOI:10.1021/jo990177f