N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

Base Information

Chemical Name:N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline
CAS No.:236111-76-5
Molecular Formula:C₂₃H₂₇N₃O₅
Molecular Weight:425.484
Hs Code.:

Synonyms:N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

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Chemical Property of N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

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Technology Process of N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

There total 5 articles about N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.7%

: 236111-75-4
N-<2-(1-azabicyclo<3.3.0>octan-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

: 236111-76-5
N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

Guidance literature:: With potassium permanganate; sodium hydrogencarbonate; In water; acetone; for 1h; Heating;
DOI:10.1248/cpb.47.880

Reference yield:

: 610-78-6
3-nitro-4-chlorophenol

: 236111-76-5
N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 91.4 percent / K₂CO₃, n-Bu₄Ni / acetone / 16 h / Heating

2: 58.2 percent / pyridine / 16 h / Heating

3: 13.7 percent / KMnO₄, NaHCO₃ / acetone; H₂O / 1 h / Heating

With pyridine; potassium permanganate; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; potassium carbonate; In water; acetone;
DOI:10.1248/cpb.47.880

Reference yield:

: 78449-78-2
7a-(2-aminoethyl)hexahydro-1H-pyrrolizine

: 236111-76-5
N-<2-(1-azabicyclo<3.3.0>octan-2-one-5-yl)ethyl>-4-(4-methoxybenzyloxy)-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 58.2 percent / pyridine / 16 h / Heating

2: 13.7 percent / KMnO₄, NaHCO₃ / acetone; H₂O / 1 h / Heating

With pyridine; potassium permanganate; sodium hydrogencarbonate; In water; acetone;
DOI:10.1248/cpb.47.880