(S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester

Base Information

• Chemical Name: (S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester
• CAS No.: 1396312-85-8
• Molecular Formula: C₂₆H₃₇N₃O₇
• Molecular Weight: 503.596

Synonyms:(S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester

Chemical Property of (S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester

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Technology Process of (S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester

There total 1 articles about (S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

L-valyl-L-phenylalanine methyl ester (39614-17-0,128557-46-0,145313-30-0) + (S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-yn-1-yloxy)propanoic acid (145205-94-3) → (S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester (1396312-85-8)

Guidance literature:

With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; In ethly acetate; at 0 - 20 ℃;

DOI:10.1055/s-0031-1291145

Reference yield: 77.0%

(11-oxo-2,3,6,7-tetrahydro-1H,5H,11H-pyrano[2,3-f]pyrido[3,2,1-ij]quinolin-9-yl)methyl azide (1396312-83-6) + (S)-2-{(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-ynyloxy)propanoylamino}-3-[methylbutanoylamino]-3-phenylpropanoic acid methyl ester (1396312-85-8) → methyl (S)-2-[(S)-2-((S)-2-tert-butoxycarbonylamino-3-{1-[(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)methyl]-1H-1,2,3-triazol-4-ylmethoxy}propanoylamino)-3-methylbutanoylamino]-3-phenylpropanoate (1396312-93-8)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In water; dimethyl sulfoxide; at 80 ℃; for 16h;

DOI:10.1055/s-0031-1291145

upstream raw materials:

L-valyl-L-phenylalanine methyl ester

(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-yn-1-yloxy)propanoic acid

Downstream raw materials:

methyl (S)-2-[(S)-2-((S)-2-tert-butoxycarbonylamino-3-{1-[(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)methyl]-1H-1,2,3-triazol-4-ylmethoxy}propanoylamino)-3-methylbutanoylamino]-3-phenylpropanoate

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