2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

Base Information

Chemical Name:2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide
CAS No.:890136-88-6
Molecular Formula:C₂₆H₂₃N₇O
Molecular Weight:449.515
Hs Code.:

2-(2-azido-phenyl)-<i>N</i>-benzyl-2-diazo-<i>N</i>-[2-(1-methyl-1<i>H</i>-indol-3-yl)-ethyl]-acetamide

Synonyms:2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

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Chemical Property of 2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

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Technology Process of 2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

There total 9 articles about 2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 890136-93-3
C₃₃H₃₁N₇O₃S

: 890136-88-6
2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ol0607138

Reference yield:

: 890136-90-0
2-(2-azidophenyl)-2-oxoacetic acid

: 890136-88-6
2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 15.0 g / acetic acid / H₂O / 3 h / 60 °C

2: 71 percent / SOCl₂ / benzene / 1 h / Heating

3: 72.6 percent / NaH / tetrahydrofuran / 1.5 h / 20 °C

4: 55 percent / triethylamine / CH₂Cl₂ / 24 h / 20 °C

With thionyl chloride; sodium hydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; benzene;
DOI:10.1021/ol0607138

Reference yield:

: 890136-92-2
2-(2-azidophenyl)-2-(tosylhydrazono)acetyl chloride

: 890136-88-6
2-(2-azido-phenyl)-N-benzyl-2-diazo-N-[2-(1-methyl-1H-indol-3-yl)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 72.6 percent / NaH / tetrahydrofuran / 1.5 h / 20 °C

2: 55 percent / triethylamine / CH₂Cl₂ / 24 h / 20 °C

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0607138