tert-Butyl (4-oxo-4-phenylbutyl)carbamate

Base Information

Chemical Name:tert-Butyl (4-oxo-4-phenylbutyl)carbamate
CAS No.:116437-41-3
Molecular Formula:C15H21 N O3
Molecular Weight:263.337
Hs Code.:2924299090
European Community (EC) Number:675-142-5
DSSTox Substance ID:DTXSID60558198
Nikkaji Number:J2.290.590B
Wikidata:Q82440402
Mol file:116437-41-3.mol

Synonyms:116437-41-3;tert-Butyl (4-oxo-4-phenylbutyl)carbamate;(4-Oxo-4-phenyl-butyl)-carbamic acid tert-butyl ester;4-(Boc-amino)-1-phenyl-butan-1-one;TERT-BUTYL N-(4-OXO-4-PHENYLBUTYL)CARBAMATE;MFCD08060130;Carbamic acid, N-(4-oxo-4-phenylbutyl)-, 1,1-dimethylethyl ester;tert-butyl 4-oxo-4-phenylbutylcarbamate;(4-oxo-4-phenyl-butyl)-carbamic acid tert-butyl;4-Oxo-4-phenyl-butyl)-carbamic acid tert-butyl ester;SCHEMBL1929771;DTXSID60558198;BAEFUAYRWLKGRC-UHFFFAOYSA-N;CS-M1642;4-(Boc-amino)-1-phenyl-1-butanone;AKOS015996762;DS-14738;SY064195;tert-Butyl(4-oxo-4-phenylbutyl)carbamate;1,1-dimethylethyl 4-oxo-4-phenylbutylcarbamate;EN300-214789;4-(Boc-amino)-1-phenyl-butan-1-one, AldrichCPR;A803619;(4-oxo-4-phenylbutyl)carbamic acid tert-butyl ester;(4-Oxo-4-phenyl-butyl)-carbamic acid tert-butylester;(4-oxo-4-phenylbutyl)-carbamic acid tert-butyl ester;F8880-3298;Z1505708866;(4-OXO-4-PHENYL-BUTYL)-CARBAMICACIDTERT-BUTYLESTER;tert-butyl N-(4-oxo-4-phenyl-butyl)carbamate

Suppliers and Price of tert-Butyl (4-oxo-4-phenylbutyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-Butyl(4-Oxo-4-phenylbutyl)carbamate
250mg
$ 90.00

SynQuest Laboratories
tert-Butyl N-(4-oxo-4-phenylbutyl)carbamate 98.0%
1 g
$ 100.00

SynQuest Laboratories
tert-Butyl N-(4-oxo-4-phenylbutyl)carbamate 98.0%
5 g
$ 397.00

Matrix Scientific
tert-ButylN-(4-oxo-4-phenylbutyl)carbamate 95%+
10g
$ 1775.00

Matrix Scientific
tert-ButylN-(4-oxo-4-phenylbutyl)carbamate 95%+
2.500g
$ 1032.00

Matrix Scientific
tert-ButylN-(4-oxo-4-phenylbutyl)carbamate 95%+
500mg
$ 514.00

Crysdot
tert-Butyl(4-oxo-4-phenylbutyl)carbamate 95+%
10g
$ 327.00

CHESS?
4-(Boc-amino)-1-phenyl-butan-1-one >98
10 g
$ 34400.00

CHESS?
4-(Boc-amino)-1-phenyl-butan-1-one >98
2 g
$ 8610.00

ChemScene
Carbamicacid,N-(4-oxo-4-phenylbutyl)-,1,1-dimethylethylester
5g
$ 167.00

Total 28 raw suppliers

Chemical Property of tert-Butyl (4-oxo-4-phenylbutyl)carbamate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:90-91°C
Refractive Index:1.507
Boiling Point:406.8°Cat760mmHg
PKA:12.66±0.46(Predicted)
Flash Point:199.8°C
PSA：55.40000
Density:1.058g/cm³
LogP:3.56510
Storage Temp.:2-8°C
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:263.15214353
Heavy Atom Count:19
Complexity:301

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl(4-Oxo-4-phenylbutyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCCCC(=O)C1=CC=CC=C1

Technology Process of tert-Butyl (4-oxo-4-phenylbutyl)carbamate

There total 8 articles about tert-Butyl (4-oxo-4-phenylbutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 85909-08-6
tert-butyl 2-oxopyrrolidine-1-carboxylate

: 100-58-3
phenylmagnesium bromide

: 116437-41-3
tert-butyl (4-oxo-4-phenyl-butyl)-carbamate

Guidance literature:: tert-butyl 2-oxopyrrolidine-1-carboxylate; phenylmagnesium bromide; In tetrahydrofuran; at -78 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield: 82.0%

: 85909-08-6
tert-butyl 2-oxopyrrolidine-1-carboxylate

: 116437-41-3
tert-butyl (4-oxo-4-phenyl-butyl)-carbamate

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.joc.1c00935

Reference yield: 76.0%

: 108-86-1,52753-63-6
bromobenzene

: 85909-08-6
tert-butyl 2-oxopyrrolidine-1-carboxylate

: 116437-41-3
tert-butyl (4-oxo-4-phenyl-butyl)-carbamate

Guidance literature:: bromobenzene; With iodine; magnesium; In tetrahydrofuran; Reflux;

tert-butyl 2-oxopyrrolidine-1-carboxylate; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1021/acs.orglett.7b01828