2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

Base Information

Chemical Name:2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)
CAS No.:1334214-69-5
Molecular Formula:C₅₈H₄₁N₅O₃Zn
Molecular Weight:921.385
Hs Code.:

Synonyms:2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

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Chemical Property of 2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

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Technology Process of 2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

There total 3 articles about 2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 179942-70-2
ethyl 6-bromo-1-ethyl-4-oxo-1,4-dihydroquinoline-3-carboxylate

: 910480-52-3
(C₆H₅)4C₂₀H₇N₄ZnBC₂O₂(CH₃)4

: 1334214-69-5
2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In N,N-dimethyl-formamide; toluene; at 80 ℃; for 16h;
DOI:10.1016/j.tet.2011.07.025

Reference yield:

: 54329-76-9
(2-bromo-5,10,15,20-tetraphenylporphyrinato)zinc(II)

: 1334214-69-5
2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride / 1,2-dichloro-ethane / 18 h / 65 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / N,N-dimethyl-formamide; toluene / 16 h / 80 °C

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tet.2011.07.025

Reference yield:

: 79607-23-1,122794-99-4
ethyl 6-bromo-4-oxo-1,4-dihydro-quinoline-3-carboxylate

: 1334214-69-5
2-(3-ethoxycarbonyl-1-ethyl-4-oxo-1,4-dihydroquinolin-6-yl)-5,10,15,20-tetraphenylporphyrinatozinc(II)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / N,N-dimethyl-formamide; toluene / 16 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; toluene; 2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tet.2011.07.025