2-bromo-5,10,15,20-tetraphenylporphinatozinc(II)

Base Information

Chemical Name:2-bromo-5,10,15,20-tetraphenylporphinatozinc(II)
CAS No.:54329-76-9
Molecular Formula:C₄₄H₂₇BrN₄Zn
Molecular Weight:757.019
Hs Code.:

Synonyms:2-bromo-5,10,15,20-tetraphenylporphinatozinc(II)

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Chemical Property of 2-bromo-5,10,15,20-tetraphenylporphinatozinc(II)

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Technology Process of 2-bromo-5,10,15,20-tetraphenylporphinatozinc(II)

There total 8 articles about 2-bromo-5,10,15,20-tetraphenylporphinatozinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2-bromo-5,10,15,20-tetraphenylporphyrin

: 557-34-6
zinc diacetate

: 54329-76-9
(2-bromo-5,10,15,20-tetraphenylporphyrinato)zinc(II)

Guidance literature:: In methanol; chloroform; at 60 ℃; for 0.5h;
DOI:10.3390/molecules25071607

Reference yield: 99.0%

: 2-bromo-5,10,15,20-tetraphenylporphyrin

: 5970-45-6
zinc(II) acetate dihydrate

: 54329-76-9
(2-bromo-5,10,15,20-tetraphenylporphyrinato)zinc(II)

Guidance literature:: In methanol; chloroform; β-tetraphenylporphyrin (240 mg) and Zn(OAc)2*2H2O (750 mg) refluxed(1 h) in CHCl3/MeOH (2:1); cooled; solvent removed (vac.); dissolved in CHCl3; chromd. (silica, CHCl3);
DOI:10.1021/jp061844t

Reference yield: 33.0%

: 14074-80-7
(5,10,15,20-tetraphenylporphyrinato)zinc(II)

: 7558-02-3,7758-02-3
potassium bromide

: 54329-76-9
2-bromo-5,10,15,20-tetraphenylporphinatozinc(II)

Guidance literature:: With ammonium molibdate; perchloric acid; dihydrogen peroxide; In dichloromethane; water; at 25 ℃; for 24h; pH=1;
DOI:10.1039/c9nj02503k