Cyclohexanecarboxamide, 2-(hydroxymethyl)-, cis- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxamide, 2-(hydroxymethyl)-, cis- (9CI)
CAS No.:116261-09-7
Molecular Formula:C₈H₁₅NO₂
Molecular Weight:157.213
Hs Code.:
Mol file:116261-09-7.mol

Synonyms:Cyclohexanecarboxamide,2-(hydroxymethyl)-, cis- (9CI); Cyclohexanecarboxamide, 2-(hydroxymethyl)-,cis-(?à)-

Suppliers and Price of Cyclohexanecarboxamide, 2-(hydroxymethyl)-, cis- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanecarboxamide, 2-(hydroxymethyl)-, cis- (9CI)

Chemical Property:

Boiling Point:357.4±11.0 °C(Predicted)
PKA:15.05±0.10(Predicted)
Density:1.095±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanecarboxamide, 2-(hydroxymethyl)-, cis- (9CI)

There total 6 articles about Cyclohexanecarboxamide, 2-(hydroxymethyl)-, cis- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89395-29-9
(3aR,7aS)-hexahydroisobenzofuran-1-one

: 116261-07-5,116261-08-6,116261-09-7
(1S,2R)-2-hydroxymethyl-1-cyclohexanecarboxamide

Guidance literature:: With ammonia; In ethanol; ethyl acetate;

Reference yield:

: 144540-72-7
trans-hexahydrophthalide

: 116174-40-4,116261-07-5,116261-08-6,116261-09-7
(1S,2S)-2-Hydroxymethyl-cyclohexanecarboxylic acid amide

Guidance literature:: With ammonium hydroxide; In toluene; for 15h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)61225-X

Reference yield:

: 65376-02-5
(1S,6R)-8-oxabicyclo[4.3.0]nonan-7-one

: 116174-40-4,116261-07-5,116261-08-6,116261-09-7
(1S,2S)-2-Hydroxymethyl-cyclohexanecarboxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: CH₃ONa / toluene / 2 h / 100 °C

2: conc. H₂SO₄ / toluene; H₂O / 2.5 h / Heating

3: NH₄OH / toluene / 15 h / Ambient temperature

With ammonium hydroxide; sulfuric acid; sodium methylate; In water; toluene;
DOI:10.1016/S0040-4039(00)61225-X