5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Base Information

Chemical Name:5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine
CAS No.:1427462-40-5
Molecular Formula:C₃₁H₃₁N₃O₁₁
Molecular Weight:621.601
Hs Code.:

Synonyms:5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Suppliers and Price of 5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

There total 10 articles about 5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 42011-36-9,59862-97-4,101685-97-6
(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(4-aminophenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 140447-00-3
2,2'-bipyridine-5-carbonyl chloride

: 1427462-40-5
5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2013.01.095

Reference yield:

: 10257-28-0
D-Galactose

: 1427462-40-5
5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 20 °C

2: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C

3: acetone / Reflux

4: hydrogen; palladium on activated charcoal / tetrahydrofuran / 20 °C

5: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

With pyridine; palladium on activated charcoal; hydrogen bromide; hydrogen; acetic anhydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2013.01.095

Reference yield:

: 25878-60-8
D-galactose pentaacetate

: 1427462-40-5
5-(-N-(p-O-(2,3,4,6-tetra-O-acetyl-β-D-galactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C

2: acetone / Reflux

3: hydrogen; palladium on activated charcoal / tetrahydrofuran / 20 °C

4: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

With palladium on activated charcoal; hydrogen bromide; hydrogen; acetic anhydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2013.01.095