2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

Base Information

Chemical Name:2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane
CAS No.:854920-60-8
Molecular Formula:C₃₈H₄₆O₄
Molecular Weight:566.781
Hs Code.:

Synonyms:2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

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Chemical Property of 2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

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Technology Process of 2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

There total 4 articles about 2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 854920-58-4
2-(3,4-bis-benzyloxy-5-bromo-phenyl)-[1,3]dioxolane

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 854920-60-8
2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

Guidance literature:: 2-(3,4-bis-benzyloxy-5-bromo-phenyl)-[1,3]dioxolane; With n-butyllithium; copper(I) bromide dimethylsulfide complex; In diethyl ether; hexane; benzene; for 0.5h;

farnesyl bromide; In diethyl ether; hexane; benzene; for 4.5h;
DOI:10.1016/j.tetlet.2005.03.187

Reference yield:

: 16414-34-9
3-bromo-4,5-dihydroxybenzaldehyde

: 854920-60-8
2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylformamide / 20 °C

2.1: pTsOH

3.1: nBuLi; CuBr*Me₂S / benzene; diethyl ether; hexane / 0.5 h

3.2: 93 percent / benzene; diethyl ether; hexane / 4.5 h

With n-butyllithium; copper(I) bromide dimethylsulfide complex; potassium carbonate; toluene-4-sulfonic acid; In diethyl ether; hexane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tetlet.2005.03.187

Reference yield:

: 100-39-0
benzyl bromide

: 854920-60-8
2-[3,4-Bis-benzyloxy-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phenyl]-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylformamide / 20 °C

2.1: pTsOH

3.1: nBuLi; CuBr*Me₂S / benzene; diethyl ether; hexane / 0.5 h

3.2: 93 percent / benzene; diethyl ether; hexane / 4.5 h

With n-butyllithium; copper(I) bromide dimethylsulfide complex; potassium carbonate; toluene-4-sulfonic acid; In diethyl ether; hexane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tetlet.2005.03.187