3,4-BIS(1-METHYLETHYL)-BENZENAMINE

Base Information

• Chemical Name: 3,4-BIS(1-METHYLETHYL)-BENZENAMINE
• CAS No.: 116233-13-7
• Molecular Formula: C12H19 N
• Molecular Weight: 177.29
• Mol file: 116233-13-7.mol

Synonyms:3,4-Diisopropylaniline

Chemical Property of 3,4-BIS(1-METHYLETHYL)-BENZENAMINE

Chemical Property:

• PSA: 26.02000
• LogP: 4.09680

Purity/Quality:

99%min ^*data from raw suppliers

3,4-BIS-(1-METHYLETHYL)BENZENAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-BIS(1-METHYLETHYL)-BENZENAMINE

There total 2 articles about 3,4-BIS(1-METHYLETHYL)-BENZENAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,4-diisopropylnitrobenzene (116233-14-8) → 3,4-diisopropylaniline (116233-13-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1021/jm00119a021

Reference yield:

1,2-diisopropylbenzene (577-55-9) → 3,4-diisopropylaniline (116233-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 81.6 percent / HNO₃, H₂SO₄ / acetic acid

2: 83 percent / hydrogen / Pd/C / ethanol

With sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In ethanol; acetic acid;

DOI:10.1021/jm00119a021

Reference yield: 61.6%

4-Methoxycarbonylbenzoyl chloride (7377-26-6) + 3,4-diisopropylaniline (116233-13-7) → methyl 4-<(3,4-diisopropylphenyl)carbamoyl>benzoate (102121-26-6)

Guidance literature:

With pyridine; In benzene; Ambient temperature;

DOI:10.1021/jm00119a021

upstream raw materials:

3,4-diisopropylnitrobenzene

1,2-diisopropylbenzene

Downstream raw materials:

4-[(3,4-diisopropylphenyl)azo]benzoic acid

methyl 4-<(3,4-diisopropylphenyl)carbamoyl>benzoate

4-[(3,4-diisopropylphenyl)carbamoyl]benzoic acid

Refernces